Electrospun Fibers for Solid-Phase Microextraction
نویسندگان
چکیده
منابع مشابه
Development of Novel Solid-Phase Microextraction Fibers
The basic principles for the preparation of SPME fibers with satisfying selectivity, sensitivity, loading capacities and stabilities are summarized here in terms of the physicochemical properties of the coating materials and the supporting substrates of SPME fibers. While the main part of this chapter focuses on the advances in developing the most widely used coating materials, including ionic ...
متن کاملSolid phase microextraction.
Solid Phase Microextraction (SPME) uses a small volume of sorbent dispersed typically on the surface of small fibres, to isolate and concentrate analytes from sample matrix. After contact with sample, analytes are absorbed or adsorbed by the fibre phase (depending on the nature of the coating) until an equilibrium is reached in the system. The amount of an analyte extracted by the coating at eq...
متن کاملIn-syringe dispersive solid phase extraction: a novel format for electrospun fiber based microextraction.
A novel in-syringe dispersive solid phase extraction (dSPE) system using electrospun silica fibers as adsorbents has been developed in the current work. A few milligrams of electrospun silica fibers were incubated in sample solution in the barrel of a syringe for microextraction assisted by vortex. Due to the benefit of dispersion and the high mass transfer rate of the sub-microscale electrospu...
متن کاملLaser Desorption Solid Phase Microextraction
The use of laser desorption as a sample introduction method for solid-phase microextraction (SPME) has been investigated in this research project. Three different types of analytical instruments, mass spectrometry (MS), ion mobility spectrometry (IMS) and gas chromatography (GC) were employed as detectors. The coupling of laser desorption SPME to these three instruments was constructed and desc...
متن کاملTheory of solid-phase microextraction
The main objective of this contribution is to describe the fundamental concepts associated with solid-phase microextraction (SPME). Theory provides insight when developing SPME methods and identifies parameters for rigorous control and optimization. A mathematical model has been developed to understand the principal processes of SPME by applying basic fundamental principles of thermodynamics an...
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ژورنال
عنوان ژورنال: Analytical Chemistry
سال: 2010
ISSN: 0003-2700,1520-6882
DOI: 10.1021/ac100891t